Innovation Center & Laboratory

Laboratory and pilot tests at UIC

For the successful realisation of your project, theoretical calculations are often not sufficient. To carry out feasibility studies and pilot tests using Thin Film, Wiped Film and Short Path distillation, a well-equipped pilot plant is available to you at our UIC headquarter in Alzenau. Here, our experts individually configure suitable laboratory and pilot plants for your distillation applications in order to develop the ideal separation process.

Decades of experience, matched with accumulated knowledge, enable us to carefully plan these tests in partnership with our customers.
The maximum flexibility of our pilot plants allows us to use numerous combinations of different components (Thin Film evaporator, Short Path evaporator, rectification column, and many more) to perform your separation task at its best.

Feasibility

The basis for a successful process solution is created in our laboratory facilities. Our units, made of glass, allow us to observe product behaviour (foaming, splashing, deposits, etc.) during distillation. These observations, together with initial analytical measurements, are essential to subsequent pilot testing and the resulting plant design. Small quantities of product (1-5 kg) are sufficient for these preliminary laboratory scale tests. For feasibility studies, both Short Path and Thin Film evaporators are available, which can also be operated in different combinations.
Depending on the product properties, we can equip our evaporators with different wiping systems.

Available technologies:

  • Thin Film evaporator type DSL5 made of glass
  • Glass rectification column operated with a Thin Film evaporator as reboiler
  • Short Path distillator type KDL5 made of glass
  • Plants can be operated individually or in combination (one or two stage distillation)
  • Melting points of operating products up to 180°C
  • Processable product viscosities up to 8,000 mPas at operating temperature
  • Various discharge systems and feed pumps available
  • Different condenser and cold trap versions available
  • Max. heating temperature for the evaporators type DSL5 & KDL5 up to 320 °C
  • Achievable operating pressure in the DSL5 Thin Film evaporator down to < 1 mbar
  • Achievable operating pressure in the KDL5 Short Path distillator down to ≤ 0.001 mbar

Scale-up

Further process development and process optimisation take place with the help of our pilot plants. Under real production conditions, the optimal throughput as well as the achievable quality and yield of a later large-scale industrial plant are determined here. Based on our scale-up trials, we provide you with a process guarantee for your customised plant.

Available technologies:

  • Thin Film evaporator type RF10 made of stainless steel
  • Short Path evaporator type KD10 made of stainless steel
  • Degasser
  • Plants can be operated individually or in combination (one or two-stage distillation)
  • Washing condenser and washing cold trap
  • Products with melting points up to 180°C can be processed
  • Products with viscosities to 8,000 mPas at operating temperature can be processed
  • Various discharge systems and feed pumps available
  • Various condenser and cold trap versions available
  • Max. heating temperature of evaporators above 350°C
  • Achievable operating pressure in Thin Film evaporator up to < 1 mbar
  • Achievable operating pressure in the Short Path evaporator up to ≤ 0.001 mbar

Entrust us with your projects and benefit from our experience and expertise

Your solution is waiting here!

Analytics

Various analytical instruments and methods are available for direct evaluation and monitoring of the tests, which are carried out by our qualified personnel.

  • Gas chromatograph (GC) with autosampler
  • Rotary viscometer
  • Aqueous and non-aqueous titrations with automatic titration systems

Further analytical methods are possible in cooperation with our customers

Confidentiality

As your reliable partner, the strictest confidentiality of your sensitive product information is of particular importance to us. As a service provider in plant engineering, we have no production or marketing interest in your products.

 

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